Comparison of mixed packing gas chromatography with mixed stationary liquid gas chromatography

Separation of Sedative – Hypnotic Drugs with Mixed Micellar Liquid Chromatography

Separation of ten sedative- hypnotic drugs was performed by RP-HPLC using mixed micellar mobile phase. Effect of temperature, type and amount of organic modifier in mobile phase on efficiency (N) and asymmetry factor (B/A) showed that, the appropriate conditions for a good separation were 35°C and 7% (V/V) butanol in mobile phase.  Variations of selectivity factor versus butanol concent...

Gas and Liquid Chromatography

Fullerene-impregnated ionic liquid stationary phases for gas chromatography.

A new method has been developed to facilitate the use of fullerenes as stationary phases (SPs) in gas chromatography (GC). In this method, ionic liquids (ILs) are used as solvents to coat fullerenes (C(60), amino-C(60) and hydroxy-C(60)) onto GC columns. However, the ILs serve not just as coating solvents but also act synergistically with fullerenes to provide unique properties as stationary ph...

Wine: Gas and Liquid Chromatography

From the chemical point of view, wines are aqueous alcoholic solutions containing more than 1000 components that can be present at high concentrations (g L ), but also at trace levels (ng L ). Some of these components determine the organoleptic properties of wines, while others are signi"cant for classifying their origin and/or for checking whether some adulteration has taken place. Concentrati...

Disopyramide determination by gas chromatography, liquid chromatography, and gas chromatography--mass spectrometry.

Disopyramide is determined in serum by gas chromatography with a nitrogen-selective detector, by liquid chromatography, and by gas chromatography--mass spectrometry. Comparable results are obtained with the three techniques, with a within-run and between-run precision of 5 to 10% (coefficient of variation). Least-squares analysis of data on patients' sera, analyzed first by gas chromatography (...